{"id":7,"date":"2017-04-06T00:18:18","date_gmt":"2017-04-06T00:18:18","guid":{"rendered":"http:\/\/nmr.sdsu.edu\/?page_id=7"},"modified":"2025-03-05T19:42:26","modified_gmt":"2025-03-05T19:42:26","slug":"home","status":"publish","type":"page","link":"https:\/\/nmr.sdsu.edu\/","title":{"rendered":""},"content":{"rendered":"

\"\"<\/strong><\/h2>\n

Overview<\/strong><\/h2>\n

The San Diego State University\u00a0NMR Facility\u00a0is a core instrumentation facility\u00a0operating under\u00a0Chemistry and Biochemistry Department at SDSU, located on the second floor of the Chemical Sciences Laboratory building, room CSL-225.<\/p>\n

Scheduling Time<\/strong><\/h2>\n

All trained users must reserve spectrometer time using the online scheduling calendar, accessed here<\/a>. \u00a0If you do not\u00a0yet have scheduling access, please\u00a0follow instructions on the Scheduler<\/a> page.<\/p>\n

Equipment<\/strong><\/h2>\n

Currently there are 4 NMR Spectrometers on site:<\/p>\n

    \n
  1. 400 MHz Varian VNMRS: Primary workhorse instrument for routine 1D and 2D liquids NMR needs. Equipped with an autosampler for overnight usage<\/li>\n
  2. 400 MHz Bruker Avance NEO Nanobay: Another workhorse instrument for routine liquids NMR needs for department researchers and undergraduate courses.<\/li>\n
  3. 500 MHz Varian VNMRS: \u00a0Overflow walkup instrument for routine NMR needs, and instrument of choice for experiments that take longer than 15 minutes.<\/li>\n
  4. 600 MHz Bruker Avance III HD: Primarily used for high-resolution and advanced liquids NMR experiments, and also for routine and advanced solid-state NMR.<\/li>\n<\/ol>\n

    Training<\/strong><\/h2>\n

    All users must be properly trained and approved by NMR Staff prior to independently using the NMR equipment. The training procedure is as follows:<\/p>\n

      \n
    1. New users should visit the New User Training page and watch the Training videos. If the page is password protected. Ask NMR Staff or lab-mates for the password.<\/li>\n
    2. After watching training videos, take the NMR Orientation \/ Safety \/ Training quiz.\u00a0 Be sure to create your NMR Scheduler account before \/ during the quiz.<\/li>\n
    3. When steps 1 and 2 have been completed, send NMR Staff an email (or visit in person) to schedule time for hands-on training.<\/li>\n<\/ol>\n

      NMR Analytical\u00a0Services for Industry<\/strong><\/h2>\n

      The SDSU NMR Facility\u00a0regularly collaborates with local industry. \u00a0Due to our simple fee-for-service setup, local companies\u00a0without in-house NMR equipment regularly request NMR analytical services from SDSU. \u00a0Common requests include: routine 1H and 13C spectra, common 2D data COSY, HSQC, HMBC, H2BC, NOESY, ROESY. \u00a0Additionally,\u00a0in many\u00a0cases we collect data on X nuclei including 31P, 19F, 11B, 29Si, etc.<\/p>\n

      Solid-state NMR capabilities can be made available to industry users\u00a0in some situations, however SDSU research projects take priority. \u00a0If you are interested in solid-state NMR data, you may need to be patient depending on instrument availability!<\/p>\n

      If you or your company are interested in NMR Analytical Services at San Diego State University, please reach out to the NMR Facility Director Dr. David Onofrei – chem-nmr@sdsu.edu. \u00a0Please include\u00a0company name\u00a0and a brief description of services requested, and we will reply shortly with a cost estimate. \u00a0Current rates for industry users: \u00a0$80\/hr for routine work, minimum 1\/2 hour. \u00a0Discounts are applied for long experiments. \u00a0Experiments are performed in-house by NMR staff, and a report will sent to the requestor via email.<\/p>\n

      Other<\/strong><\/h2>\n

      Department Gas and Liquid Nitrogen orders are handled by Laura Cervini. \u00a0Orders must be placed every MONDAY<\/strong> for Wednesday delivery.<\/p>\n

      Link to order gas and LN2:
      \nhttps:\/\/docs.google.com\/forms\/d\/1Qof793psNcmfZLgCDY1XoLOJDexs5w6c2rXSDRKmPSU\/viewform?pli=1&ts=64a5fb20&pli=1&edit_requested=true<\/a><\/p>\n

      Link to view status of order:
      \n      https:\/\/docs.google.com\/spreadsheets\/d\/1q1YFkA1Ea6Bz_I7mc2SJV_T7Jpv_wsYo2Mn6sSZB-kQ\/edit?usp=sharing<\/a><\/p>\n","protected":false},"excerpt":{"rendered":"

      Overview The San Diego State University\u00a0NMR Facility\u00a0is a core instrumentation facility\u00a0operating under\u00a0Chemistry and Biochemistry Department at SDSU, located on the second floor of the Chemical Sciences Laboratory building, room CSL-225. Scheduling Time All trained users must reserve spectrometer time using … Continue reading →<\/span><\/a><\/p>\n","protected":false},"author":1,"featured_media":27,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":""},"class_list":["post-7","page","type-page","status-publish","has-post-thumbnail","hentry"],"_links":{"self":[{"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/pages\/7","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/comments?post=7"}],"version-history":[{"count":26,"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/pages\/7\/revisions"}],"predecessor-version":[{"id":357,"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/pages\/7\/revisions\/357"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/media\/27"}],"wp:attachment":[{"href":"https:\/\/nmr.sdsu.edu\/index.php\/wp-json\/wp\/v2\/media?parent=7"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}