In this section, you will find screen-recorded videos and brief explanations of key NMR concepts and how to operate the NMR equipment for advanced use cases. It is advised that you go through these videos in order, since later videos will reference earlier videos. These videos were recorded by Dr. Bennett Addison. Email for comments / suggestions on additional content!
Getting Started: First, you should know how to operate the instruments in standard “Study Queue” mode.
Operating 400 and 500 in Study Queue Mode – Routine Proton
Operating NMR400 using Autosampler
- Manual locking, manual shimming, trail spectra
- Manual probe tuning
- Basic NMR Acquisition Parameters
- T1 Relaxation – Concepts, data acquisition, data analysis
- Common Problem – Artifacts from too much signal
- Advanced 1D Experiments (1D Homodec, Wet1D, 1D NOE, DEPT, etc)
- Common 2D NMR (COSY, HSQC, HMBC) for organic structure characterization
